Weekly Questions and Answers

By George Trigg, GRT Engineering
and Nick Liberto, Powder Coating Consultants

Welcome to Powder Coating magazine's Weekly Questions & Answers column. Questions for this column are submitted by powder coaters just like you who are seeking ways to improve efficiencies and solve every day problems on their powder coating lines.

4/13/2015 - Q: I have a customer who is asking about the performance of powder coating at -40°F. We’re coating coil springs (high carbon steel) that are cleaned before powder coating through an aggressive shot peen necessary for spring properties. We currently are using silver TGIC-based (triglycidyl isocyanurate) polyester with a full-gloss, clear TGIC-based polyester topcoat. Have powder coatings ever been tested at such extreme temperatures? Any educated guess as to what would happen at this temperature? The customer is being rather evasive about the specific end use. I appreciate any light you can shed on this issue. P.M., Pittsburgh, Pa.

A: In one of my former lives, I worked in the appliance industry. We installed one of the first major automated powder systems for refrigerator liners, which is the interior shell of a refrigerator. This liner is designed to include the freezer portion of the unit. Temperatures in a freezer compartment can reach nearly zero, depending on the setting by the homeowner. We had absolutely no problems. We deliberately flexed the metal to see if we lost adhesion, and everything was OK. Now, I hasten to add that these units are sheet metal and not spring steel; they don’t see daily flexing such as a spring might. I tried cryogenic hook cleaning for a system that I installed, also in the appliance industry. This is a process that was being promoted by a large supplier of the gases used in this process. Couldn’t touch the powder on the hanger. Parameters were about 3 mils of powder; time ranged from a few minutes up to just short of an hour. At about an hour, we saw some cracking and crazing of the outer coating, but it wouldn’t peel from the hanger, even with a hammer blow. This process has been used on liquid paint, at fairly low film, and works. I don’t know how well it works over time. think it’s interesting that you need to put a high-gloss clear over a metallized first coat on a spring. Oh well, none of my business. I sure wouldn’t do anything unless I tested it first. One concern would be the inner-coat reaction between the clear and the silver. The other is, of course, can the coating flex along with the spring steel. Having been intimate with the refrigerator tests, I’m inclined to say it will work OK, at least for a time. Constant flexing, day in and day out, may be something else. I queried a technical director for one of the larger powder coatings suppliers who said that unless the clear is formulated for 0-T, which means the capability to withstand a sheet metal bend back on itself, it’ll craze when the spring does a tight compression. I wouldn’t commit to anything until the customer revealed some additional information. —G.T.

4/6/2015 - Q: I coated a fancy decorative metal piece with a polyester clear that bonded with aluminum. I decorated it in the backyard. It got wet during the last rain, which changed the appearance. It looks like the aluminum oxidized. It looks darker. Is there any way I can restore its original color by cleaning with alcohol or another cleaner? I really appreciate you answer. P.R., Midland, Tex.

A: At what temperature did you cure the clear coat? Aluminum forms a self-protective coating that acts as a preservative. If you didn’t clean that off just before painting, then you will not have any adhesion. If that’s so, then moisture likely got between the clear coat and the aluminum. If the coating was cured at its recommended temperature, alcohol won’t remove it, even with poor adhesion. What may happen if the adhesion is poor? If you try to remove the paint with a mild solvent, some of it will come off and some of it won’t. You need a much stronger solvent, like methylene chloride (MC) or methyl ethyl ketone (MEK), but both of these are nasty to work with manually. Take the proper precautions. If you live near one of the larger cities, try to find a company that does stripping and have them do it for you. It’ll cost a little bit, but it’ll be so much easier than hand stripping. —G.T.

3/30/2015 - Q: I work for a recreational company, and we powder coat many different items within an order. This may be 10 to 100 different tube lengths, but these tubes are scattered throughout the line depending on the color. My question is, what's the best way to identify parts before they get coated and then be able to identify them at the packing end of the line? M.U., Lewisburg, Pa.

A: Well, let's try this. You can use a metal tag maybe the size of a quarter or whatever, depending on how you identify the various parts. Affix this tag to a small magnet, and place it on the rack or wire that holds the parts. When the parts are unloaded (cool I presume), place the tag on the part. At the packing end, remove the metal tag. Caution here: The cure heat will shorten the service life of the magnet, and that metal will need to be remagnetized in the near future. Maintenance can set this up for you. I haven't a clue as to how you handle the parts through your shop, but another way is to use the tag system on the rack but shielded from powder spray. After cure, use a tie wrap on the finished part, which will have the metal tag hanging from it. Again, shipping people can remove this tag and send it back for reuse. Not knowing what the parts look like limits my assistance. Are there assembly holes available? Are these open-ended tubes? If so, you have a lot of possibilities to identify parts. —G.T.

3/23/2015 - Q: We are powder coating aluminum dock ladders in candy colors from TIGER Drylac. We are having problems with the powder peeling off in sheets as well as poor uniformity in the color throughout each ladder. We wash each part with a degreaser and then rinse it with softened water. Next, we use an acid cleaner to etch the part and then rinse it again with softened water. How do we stop the powder problems in the future? R.P., Jamestown, Ohio

A: Powder coating aluminum poses special challenges not normally seen when dealing with ferrous substrates. First of all, aluminum readily oxidizes when exposed to air, causing aluminum oxide on the surface (white powdery residue). Of course, ferrous substrates will also oxidize in air, but the oxidation (red rust) is more easily seen before coating and therefore can be removed before it causes a problem. This is the reason you are using an acid etchant to remove this oxide as the final step in preparing your parts. A second issue that is somewhat unique to aluminum is that the surface of extrusions are remarkably smoother than ferrous parts. This surface smoothness means reduced adhesion as the coating requires good surface “tooth” for the coating to “bite” onto. Often, aluminum parts are chemically conversion coated (using either zirconium or chromate) to provide both better surface “tooth” and improved corrosion resistance. Of course, you can rough-up the surface using Scotch pads or sandpaper to improve the “tooth”. A third issue that causes poor adhesion and low corrosion resistance is rinse water quality. You mentioned that you use “softened” water to rinse the parts. While softened water is suitable for household use, it is less desirable for metal surface preparation prior to powder coating. The water softening process uses salts to remove/neutralize the hardness contaminants. These salts can leave a residue on the surface if not properly balanced. The residue prevents proper coating adhesion. Using a DI or RO water process will provide suitable quality water and eliminate the problem associated with water softening systems. Finally, undercured powder coating will be exhibited as poor adhesion to the substrate. Ensure that you are fully curing the products using the PCI Solvent Cure Test Procedure #8. —N.L.

3/16/2015 - Q: Do you have any information on electrical bus bar insulation by fluidized epoxy coatings? I’m looking into what’s required for the process and technical specs on the base material. J.C., Holland, Mich.

A: Bus bars are coated via fluidized bed by some very large companies. It’s fairly easy, depending on the size of the bus bar. Epoxy is a good choice because it has some insulating factor, but be aware that it chalks if used in sunlight. Contact a reputable powder coatings supplier for the material you need. You should consider heating the bar before spraying to get maximum film build. You can do this with induction heating, or, if you’re on a tight budget, with an oven. The nice thing about induction heating is you preheat, coat, water quench, and then load right on the truck. No hands except to load it on the truck. Fluid-bed applications will work on straight-line bus bar, but "dog leg" or contoured bus will present a problem. —G.T.

3/9/2015 - Q: We’re now producing an outdoor part (steel or aluminum) with a five-stage zinc phosphate pretreatment finish and a polyester powder coating topcoat. I want to know for both substrates if a mechanical pretreatment such as sandblasting is as good as our chemical pretreatment. Also, what is the best way to finish these parts? Apply a thicker topcoat (if yes, how much?) or use a powder primer before. C.F., Notre-Dame-du-Bon-Conseil, Que.

A: Zinc phosphate pretreatment is just about the ultimate chemical pretreatment for metal. For aluminum however, I wouldn’t call it overkill, just a bit wasteful. It will not hurt, and if the line is set up for all metals, then fine, go with it. I can’t accurately tell what the best metal cleaning and preparation is for your system without knowing what it is you expect the coating to do in the field. Blasting works well for some products, not so well for others. If you have a moisture issue when the parts are in use by your customer, then the added benefit of chemical pretreatment will certainly help adhesion and inhibit corrosion. If that isn’t an issue, then you may wish to look at and test media blasting and powder coating. Depending on end use, you might consider a two-coat system: Media blast, zinc primer, then polyester topcoat. You know that media blasting might alter the surface of the metal, depending on what it has to remove from the metal and on the type of media material you use. Powder coatings manufacturers design powder coatings for certain film thicknesses. Applying the material heavier than recommended will lead to a negative result, and thicker won’t solve an adhesion problem. If you think you could have field failures due to atmospheric conditions, then a two-coat system would work well. And as I mentioned, if you go that route, you could media blast and not use chemical pretreatment. Of course, you probably wouldn’t want to use the same media particle size or material on the aluminum that you would use on the ferrous metal. —G.T.

3/2/2015 - Q: A new customer discussed a problem he had with his old powder coater. He explained that his old guy only processed his oven time at 30 minutes max no matter how thick the material was. How can I best explain to him how the finished product will be with under-heating? I’ve only been in business for 1 year and am still learning myself. B.S., Yucca Valley, Calif.

A: At the risk of getting extreme, the proper method of curing is to know what the metal is doing. If the powder coating is scheduled to be cured at 360°F for 10 minutes, then that’s what you need. If you don’t have any idea what the part temperature is, you’ll have cure all over the chart. Thirty minutes at some temperature is pretty safe from some aspects, but it could be grossly over-curing the part. If the parts are heavy castings, or in other words, heat sinks, they could be under-cured, which would be the worst of the two conditions. If the former coater has been doing this for a long time, he can probably get fairly close to time and temperature by experience alone. However, to arbitrarily cure everything for 30 minutes? I wouldn’t want him coating my parts! —G.T.

2/23/2015 - Q: How do I calculate the heat load for a powder curing convection oven? Is there a relation between heat load and the circulating fan? If yes, what is the relation? A.H., Bangalore, Karnataka, India

A: This information is contained in various articles I’ve written over the years in this publication. (See the Article Index at www.pcoating.com; click on Authors and scroll to L. You’ll find the articles listed under my name.)

As I’m not in favor of helping unqualified persons from designing equipment that can cause injury or death when it fails, I’ll provide my answer in engineering terms and not provide the actual formulas. My liability insurance company is very comfortable with this personal and professional choice. I hope that you are as well.

The heat load for a convection cure oven is determined by the mass of the products to be cured multiplied by the specific heat of the substrate. This value is then multiplied by the delta temperature (room temperature to cure temperature). The mass of the hangers and conveyor chain must be added to this calculation in conveyorized systems. In addition, the radiant heat loss through the oven walls must be included in the heat load. Finally, the heat lost through the exhaust fan and stack must be included, as well.

Any well-designed convection oven must deliver the BTU energy from the burner efficiently to the parts through the use of a properly sized circulation fan. The circulation fan must provide at least three turns per minute to be efficient, but more is better.

My recommendation is that you use this information to judge an oven design from a qualified equipment supplier and not design your own oven. The consequences of doing the oven design incorrectly range from using too much energy or not properly curing your parts to having to rebuild your plant after the explosion and paying for the funerals of your shop personnel.—N.L.

2/16/2015 - Q: I’m using an alkaline cleaner on two different lines. On one of the lines, I’m able to run it at 110°F; however, on the other line, I’m unable to run below 140°F as it foams madly. What could be checked to remedy this foaming so that I can run the stage at 110°F like the other line? K.M., Holland Landing, Ont.

A: If we assume that both lines are identical mechanically, the only logical reason is that you’re trying to remove a different soil on the foaming line. Conduct a soil and substrate audit for both lines. What soils are applied to the metal before processing? You may find that a fatty acid soil or an animal fat lube is being applied to the metal. This creates saponification when a heated especially caustic containing cleaner is used. You create "soap" and thus foaming. If this is the case, change soils. Also ask the chemical supplier this: What is the cloud point of the surfactant system in use with my cleaner? My guess is that he’ll say 110°F to 115°F. —G.T.

2/9/2015 - Q. Are there any specific quality issues or process requirements a powder coater needs to be aware of when powder coating over Zintec mild steel? I’m a buyer in the middle of a sheet metal producer in England, who uses Zintec to manufacture parts for us, and a powder coater in the US, who will eventually coat the parts. I realize the question is so general that the answers may be limitless. Any help in pointing me to resources would be appreciated. J.W., Lincolnwood, Ill.

A: Zintec is a brand of zinc-coated steel similar to Galvanneal, galvanized, or aluminized steel. Depending on the coating performance specifications, a zinc phosphate pretreatment would give the best results although it’s not uncommon to use iron phosphate. You should be aware that you can get outgassing from these types of substrates during the cure cycle for the powder. Often, preheating the part will reduce or eliminate the problem. Heavy powder film build can also inhibit the gasses from getting to the surface. You might want to make sure the supplier in England doesn’t coat the parts in a heavy rust preventive for resistance to oxidation when shipping by boat. A heavy coating of oils and so on will make it difficult for your US coater, and you will end up in a finger-pointing contest. The shipper would be most helpful by using a watertight container and maybe some desiccant drying materials. —G.T.

2/2/2015 - Q: We’re considering an expansion of our powder coating room, and questions have arisen regarding the need for explosion proofing. Are there any general guidelines available that we can consult for information regarding what, if any, regulations there may be for explosion proofing that we have to abide by in this project? M.B., Oak Creek, Wis.

A: Check with National Fire Protection Association (NFPA) codes, Chapter 33, which are the generally accepted requirements for safety items. However, you should also check local codes with your community fire marshal. The NFPA codes are adequate, but many times the locals insert their own requirements, which can be more stringent than NFPA's. A powder booth must be explosion vented. Some requirements demand that it be vented to the outside. Some just require that you vent to an unoccupied area, such as a high ceiling. This can cause you to modify your application system layout, so check this carefully. In smaller communities, you can find all kinds of variances in the codes. Some fire marshals (inspectors) don’t have any idea what constitutes a powder coating system and will demand that you meet wet paint regulations. If you get a hardheaded inspector, you’re in for a real treat, so it’s best to review what you’re doing before you do it. Maybe that will be the last and only time you hear from that person. —G.T.

1/26/2015 - Q: What powder coating and cleaning process do you recommend for corrugated brass tubes? These brass tubes are used for gas connectors and need to be ammonia-resistant. T.M., Rancho Cucamonga, Calif.

A: The powder of choice is a triglycidyl isocyanurate-based (TGIC-based) polyester, I believe. That’s the easy part. The cleaning step is a little different. A similar project that I worked on used different tubing. This stainless steel tubing was annealed for improved flexibility, and the annealing burned away any oils or impurities on the metal. As a result, they didn’t pretreat the tube. They just applied the powder. I don’t know what you’re doing with the tube you manufacture. If you’re annealing, then don’t do anything else. If you’re not annealing, then some type of pretreatment would certainly improve adhesion. Chemically pretreating will be difficult with the tube already corrugated. Powder coating with the parts hanging horizontally works best. If you hang vertically, the parts will sway and bump into each other (wind-chime) and cause defects and line wrecks. However, pretreating horizontally will cause a lot of dragout. You probably have that all figured out. If there is any kind of contamination on the parts, you’ll lose adhesion, and for this part, which needs to flex, you certainly don’t want adhesion loss. This material is a bit tricky. Be sure you look in the valleys of the corrugating, using a glass, because the paint may crack so fine that you won’t see it with the naked eye. But it will certainly be a failure. If you need additional help with the pretreatment, send me a more detailed description of how you’re now cleaning. —G.T.

1/19/2015 - Q: We currently have three powder lines. All three use a cartridge reclaim system. We have been running the same recycled powder for an unknown amount of time. To my knowledge, we have never actually dumped powder and started with new on some colors. Thus, the particle size ranges are affecting the chargeability of the powder and in turn affecting the transfer efficiency (TE). When should I take a stand, so to speak, to reduce this effect? Could this also be affecting the amount of powder that is escaping from the booths? Any input you can offer would be taken on board with thanks! J.A., Zhongshan, Guangdong Province, China

A: With some slight reservation, I say it’s time to take a stand. My reservation is that poor part design, that is, a part not designed with painting in mind, can affect the outcome, but you probably can’t do anything about that. It seems from here that poor TE is the problem, maybe not the root of the problem, but nonetheless a problem. You know that the reclaim is out of whack, but the guy who pays the bills probably doesn’t--and doesn’t care. But poor TE is costing you money and time, which is still money. You’re right in that the smaller the particle size, the poorer the chargeability of the powder and the more difficult it is to get the required film on the parts. Eventually, you’ll have no fluidization, or at best you’ll have to jumpstart the fluidization with a paddle or some such device. You might be able to help by redesigning the hangers so that they will present the parts to the application equipment in a better way to increase powder transfer. You should study this and be prepared to offer some ideas when the boss asks what you propose to do to fix the situation. Yes, poor TE and reclaim overuse (which will increase small particles) can result in powder escaping the booth. Part of that problem is likely caused by the small particles clogging the filters. Take an airflow reading at the part openings. If it’s low, as I suspect, that will also cause powder drifting. This costs money and makes for a messy shop. So, you need to install new filters, remodel the hangers, dump the powder now in the hoppers, and realign the guns for better coverage. If the boss doesn’t want to do any of these things, you should look for another job where they will appreciate your understanding of powder applications. —G.T.

Further reading on the problems discussed in this column can be found in our Article Index and Bookstore.

George R. Trigg is president of GRT Engineering, 6314 Hughes Road, Prospect, OH 43342; 740/494-2496. He has been involved in the powder coating industry for more than 38 years. He holds a BSBA degree from Muskingum College, New Concord, Ohio. His email address is molly95@earthlink.net.

Nick Liberto is president of Powder Coating Consultants (www.powdercc.com), a division of Ninan Inc., 1529 Laurel Avenue, Bridgeport, CT 06604; 203/366-7244. He has more than 3 decades of experience in the powder coating industry. A registered professional engineer in Connecticut, he holds a bachelor’s of science degree in mechanical engineering with a minor in physics. His email address is pcc@powdercoat.com.

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